1 Sentences With "over reduce"

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Care must be taken to not over reduce the silicon; often triethylamine is added to prevent over reduction. The yield for this reduction can be as high as 80%. N-heterocyclic silylenes containing Silicon(II) with four-membered rings (1 carbon) and six- membered rings (3 carbons) are well known and derived from the reactions of SiX4 with amidinate and NacNac ligands respectively. The silylenes synthesized prior to West and Denk's first NHSi decomposed at temperatures below 77K.